Introduction

Common extraction techniques for solid matrices include Soxhlet extraction, sonication extraction, supercritical fluid extraction (SFE), microwave-assisted extraction (MAE), and accelerated-solvent extraction (ASE).

Soxhlet extraction allows use of large amount of sample (e.g. 10-30 g), no filtration is required after the extraction, the technique is not matrix dependent, and many Soxhlet extractors can be set up to perform in unattended operation. The most significant drawbacks of Soxhlet extraction are: long extraction times (e.g. up to 24-48 h), large amount of solvent usage (300-500 mL per sample), and the need for evaporation after sample extraction.

Sonication extraction is faster than Soxhlet extraction (30-60 min per sample) and allows extraction of

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large amount of sample with a relatively low cost, but it still uses about as much solvent as Soxhlet extraction, is labour intensive, and filtration is required after extraction.

The newer extraction techniques such as SFE, MAE, and ASE are very attractive because they are a lot faster, use much smaller amounts of solvents, and are environmentally friendly techniques. For example, SFE uses carbon dioxide or modified carbon dioxide (e.g., carbon dioxide containing a small amount of an organic solvent known as modifier) for extraction. Carbon dioxide is a nontoxic, nonflammable, and environmentally friendly solvent. Furthermore, the extraction selectivity can be controlled by varying the pressure and temperature of the supercritical fluid and by the addition of modifiers.

MAE uses microwaves that can easily penetrate into the sample pores causing the solvent trapped in the pores to heat evenly and rapidly. In contrast to conventional heating where it takes a long time for the vessel to heat and then transfer its energy to the

Solar Panel Basics

Solar Panel Basics

Global warming is a huge problem which will significantly affect every country in the world. Many people all over the world are trying to do whatever they can to help combat the effects of global warming. One of the ways that people can fight global warming is to reduce their dependence on non-renewable energy sources like oil and petroleum based products.

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